Determination of titanium content in pyrotechnics used for fireworks and firecrackers based on Energy Dispersive X-ray Fluorescence Spectrometry (EDXRF)
Jun-yi Wu, Huan-xin Xiao
Available Online April 2017.
- https://doi.org/10.2991/fmsmt-17.2017.3How to use a DOI?
- fireworks and firecrackers;pyrotechnics;titanium content; determination; Energy Dispersive X-ray Fluorescence Spectrometry;EDXRF.
- Methods used for the determination of titanium content in pyrotechnics are mostly based on traditional chemical method, which is lengthy and cumbersome. If inductively coupled plasma emission spectrometry or atomic absorption spectrometry are used to determine the titanium with high content,the sample solution must be highly diluted,and it mustproduce errors in measurement and calling into question the reliability of the data.The method mentioned in this paper is about the determination of titanium content in pyrotechnics used for fireworks and firecrackers based on energy dispersive X-ray fluorescence spectrometry by controlling matrix effects between elements.Using samplesolution of pyrotechnics in specific concentrates,the titanium content can be determinedby the specificcalibration curve established with an intensity calibration.This method can provide high accuracy and good precision in a short time with a simple process byefficiently controlling the matrix effects.It can fully meet the requirements forthe determination of titanium in pyrotechnicsused for different kinds of fireworks and firecrackers around the world,and ithas good generalization and practicability.The average recovery of the method can be98.88%~100.56%, allowing for a difference of 0.5%.
- Open Access
- This is an open access article distributed under the CC BY-NC license.
Cite this article
TY - CONF AU - Jun-yi Wu AU - Huan-xin Xiao PY - 2017/04 DA - 2017/04 TI - Determination of titanium content in pyrotechnics used for fireworks and firecrackers based on Energy Dispersive X-ray Fluorescence Spectrometry (EDXRF) BT - Proceedings of the 2017 5th International Conference on Frontiers of Manufacturing Science and Measuring Technology (FMSMT 2017) PB - Atlantis Press SP - 12 EP - 17 SN - 2352-5401 UR - https://doi.org/10.2991/fmsmt-17.2017.3 DO - https://doi.org/10.2991/fmsmt-17.2017.3 ID - Wu2017/04 ER -