Proceedings of the 2017 5th International Conference on Frontiers of Manufacturing Science and Measuring Technology (FMSMT 2017)

Determination of lead content in pyrotechnics used for fireworks and firecrackers based on inductively coupled plasma optical emission spectrometric approach (ICP-OES)

Authors
Jun-yi Wu
Corresponding Author
Jun-yi Wu
Available Online April 2017.
DOI
https://doi.org/10.2991/fmsmt-17.2017.79How to use a DOI?
Keywords
fireworks and firecrackers; pyrotechnics; lead content; determination; inductively coupled plasma optical emission spectrometric approach; ICP-OES.
Abstract

Inductively coupled plasma optical emission spectrometric approach(ICP-OES) is used to determine the lead content in pyrotechnics used for fireworks and firecrackers. Element of lead is commonly found as impurity in chemical materials used for pyrotechnics in fireworks and firecrackers. Statistical analysis shows that lead content in pyrotechnics is below 5%.Concept of this method: considering the weight of the sample is 400mg,constant volume is 0.5L and the concentration of lead is below 40mg/L in sample solution, the determination scope of the method for the lead content would be between 5%.Further experiments proved that the fitting correlation coefficient of lead calibration curve is 0.9997 or higher, recovery is 92.53%-115.63%.The allowable differential value is 0.4% between two single tests under repeatable conditions. This method can completely satisfy the requirements of the fireworks and firecrackers industry with high accuracy and good precision.

Copyright
© 2017, the Authors. Published by Atlantis Press.
Open Access
This is an open access article distributed under the CC BY-NC license (http://creativecommons.org/licenses/by-nc/4.0/).

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Volume Title
Proceedings of the 2017 5th International Conference on Frontiers of Manufacturing Science and Measuring Technology (FMSMT 2017)
Series
Advances in Engineering Research
Publication Date
April 2017
ISBN
978-94-6252-331-9
ISSN
2352-5401
DOI
https://doi.org/10.2991/fmsmt-17.2017.79How to use a DOI?
Copyright
© 2017, the Authors. Published by Atlantis Press.
Open Access
This is an open access article distributed under the CC BY-NC license (http://creativecommons.org/licenses/by-nc/4.0/).

Cite this article

TY  - CONF
AU  - Jun-yi Wu
PY  - 2017/04
DA  - 2017/04
TI  - Determination of lead content in pyrotechnics used for fireworks and firecrackers based on inductively coupled plasma optical emission spectrometric approach (ICP-OES)
BT  - Proceedings of the 2017 5th International Conference on Frontiers of Manufacturing Science and Measuring Technology (FMSMT 2017)
PB  - Atlantis Press
SP  - 374
EP  - 379
SN  - 2352-5401
UR  - https://doi.org/10.2991/fmsmt-17.2017.79
DO  - https://doi.org/10.2991/fmsmt-17.2017.79
ID  - Wu2017/04
ER  -