Synthesis and characterization of poly (Itaconic Acid-m-Phen- ylenediamine)

DOI

10.2991/imst-16.2016.3How to use a DOI?

Keywords

low temperature solution polycondensation; itaconyl chloride; polymer; inherent viscosity; characterization.

Abstract

With Itaconyl chloride and m-phenylenediamine as raw materials, poly(itaconic acid- m-phenylenediamine) was synthesized by the low temperature solution polycondensation we reported. The effects of initial temperature and reaction time on polycondensation were investigated. And the product was characterized by 1H-NMR, FT-IR and TGA. The results showed that the polycondensation should carry out at a low temperature. The initial temperature should be lower 0 °C. The polycondensation time was 90-100 minutes. Under these conditions, the thermal stability was good and its inherent viscosity was about 1.4. The spectra of FT-IR and 1H-NMR confirmed its structure.

Copyright

© 2016, the Authors. Published by Atlantis Press.

Open Access

This is an open access article distributed under the CC BY-NC license (http://creativecommons.org/licenses/by-nc/4.0/).

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TY  - CONF
AU  - Chuanxing Wang
AU  - Pengfei Wang
AU  - Qinhong Xu
AU  - Zhe Wei
AU  - Yumin Wu
PY  - 2016/11
DA  - 2016/11
TI  - Synthesis and characterization of poly (Itaconic Acid-m-Phen- ylenediamine)
BT  - Proceedings of the 2016 International Conference on Innovative Material Science and Technology (IMST 2016)
PB  - Atlantis Press
SP  - 18
EP  - 24
SN  - 1951-6851
UR  - https://doi.org/10.2991/imst-16.2016.3
DO  - 10.2991/imst-16.2016.3
ID  - Wang2016/11
ER  -