Synthesis and Characterization of (-)-Dibornyl Oxalate
Xiaomin Yuan, Zhendong Zhao, Shichao Xu, Yuxiang Chen, Liangwu Bi
Available Online August 2015.
- https://doi.org/10.2991/ic3me-15.2015.86How to use a DOI?
- (-)-Borneol, Oxalyl Chloride, (-)-Dibornyl oxalate, Characterization
- (-)-Dibornyl oxalate was synthesized by the reaction of natural (-)-borneol with oxalyl chloride under the optimized reaction conditions: temperature 35 , time 1 h and the molar ratio of (-)-borneol and oxalyl chloride 1.0 : 0.6. The reaction underwent in good selectivity as 99 % for target product which can be easily purified to 99.9 % through recrystallization. The structure of (-)-dibornyl oxalate was characterized by GC-MS, FT-IR, 1H NMR and 13C NMR.
- Open Access
- This is an open access article distributed under the CC BY-NC license.
Cite this article
TY - CONF AU - Xiaomin Yuan AU - Zhendong Zhao AU - Shichao Xu AU - Yuxiang Chen AU - Liangwu Bi PY - 2015/08 DA - 2015/08 TI - Synthesis and Characterization of (-)-Dibornyl Oxalate BT - 3rd International Conference on Material, Mechanical and Manufacturing Engineering (IC3ME 2015) PB - Atlantis Press SN - 2352-5401 UR - https://doi.org/10.2991/ic3me-15.2015.86 DO - https://doi.org/10.2991/ic3me-15.2015.86 ID - Yuan2015/08 ER -