Study on the determination of sodium cyclamate in the jelly

DOI

10.2991/meic-15.2015.65How to use a DOI?

Keywords

sodium cyclamate;jelly;high efficiency liquid chromatography;detection

Abstract

Objective: In order to study the contect of sodium cyclamate in jellies. Method: Using ring amino sulfonate sodium hypochlorite derived reaction occurs under acidic conditions to generate N-,N-dichloro-cyclohexane,and then hexane extracted ODC-C14 column,methanol(V):water(V)=80:20 as mobile phase separation,the flow rate was 1.0mL/min, the injection volume was 20ul,the detection wavelength of 314nm.Result This high-efficiency liquid chromatography determination of the concentration of sodium cyclamate in the linear relationship between the 0-300ug/ml,the correlation coefficient was 0.9995 above, and require accuracy and good reproducibility. The recovery rate of sodium cyclamate was 80%-120%,the coefficient of variation less than 10%.Conclusion:The method is rapid, simple,highly sensitive and with less interference, which is suitable for the detection of cyclamate in jellies.

Copyright

© 2015, the Authors. Published by Atlantis Press.

Open Access

This is an open access article distributed under the CC BY-NC license (http://creativecommons.org/licenses/by-nc/4.0/).

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TY  - CONF
AU  - Boru Ren
AU  - Na Liu
AU  - Jie Zhao
AU  - Tingxin Wang
PY  - 2015/04
DA  - 2015/04
TI  - Study on the determination of sodium cyclamate in the jelly
BT  - Proceedings of the 2015 International Conference on Mechatronics, Electronic, Industrial and Control Engineering
PB  - Atlantis Press
SP  - 273
EP  - 276
SN  - 2352-5401
UR  - https://doi.org/10.2991/meic-15.2015.65
DO  - 10.2991/meic-15.2015.65
ID  - Ren2015/04
ER  -