Synthesis o f Ti2N Powders by Vacuum Slowly Vapor Deposition Using Urea as Nitrogen Source
- https://doi.org/10.2991/meep-15.2016.36How to use a DOI?
- urea; TiCl3; vacuum slow deposition; TiN
Hydrochloric acid solution of TiCl3 was synthesized by reacting of Ti powders and hydrochloric acid in highpressure reactor at 145 . After vacuum drying TiCl3·6H2O crystalline were obtained. TiCl3·6H2O crystalline and urea, being as nitrogen source, were put into the vacuum slowly vapor deposition reactor. The heating temperature and holding time were 600 and 10 min separately. The deposited powders at different temperature were analyzed by X-ray diffraction (XRD). The results show: Ti2N powders can be synthesized at the range of 450 to 600 . The powders deposited at low temperature ( 80 ) were NH4Cl and the organics decomposed from urea.
- © 2016, the Authors. Published by Atlantis Press.
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- This is an open access article distributed under the CC BY-NC license (http://creativecommons.org/licenses/by-nc/4.0/).
Cite this article
TY - CONF AU - J.F. Sun AU - S. Yan AU - H. Yu AU - K. Quan PY - 2016/03 DA - 2016/03 TI - Synthesis o f Ti2N Powders by Vacuum Slowly Vapor Deposition Using Urea as Nitrogen Source BT - Proceedings of the 2015 International Conference on Materials Chemistry and Environmental Protection (meep-15) PB - Atlantis Press SP - 136 EP - 138 SN - 2352-541X UR - https://doi.org/10.2991/meep-15.2016.36 DO - https://doi.org/10.2991/meep-15.2016.36 ID - Sun2016/03 ER -